Optimizing NMR Methods for Structure Elucidation: Characterizing Natural Products and Other Organic Compounds
Author:   Darcy C Burns (University of Toronto, Canada) ,  William F Reynolds (University of Toronto, Canada)
Publisher:   Royal Society of Chemistry
Volume:   Volume 17
ISBN:  

9781782625391


Pages:   256
Publication Date:   28 September 2018
Format:   Hardback
Availability:   In Print   Availability explained
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Optimizing NMR Methods for Structure Elucidation: Characterizing Natural Products and Other Organic Compounds


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Overview

This book is aimed at informing organic chemists and natural products chemists on the use of NMR for structure elucidation to enable them to ensure they yield the most reliable possible data in the minimum possible time. It covers the latest pulse sequences, acquisition and processing methods, practical areas not covered in most texts e.g. detailed consideration of the relative advantages and disadvantages of different pulse sequences, choosing acquisition and processing parameters to get the best possible data in the least possible time, pitfalls to avoid and how to minimize the risks of getting wrong structures. Useful in industrial, pharma or research environments, this reference book is for anyone involved with organic chemistry research and, in particular, natural products research requiring advice for getting the best results from the NMR facilities.

Full Product Details

Author:   Darcy C Burns (University of Toronto, Canada) ,  William F Reynolds (University of Toronto, Canada)
Publisher:   Royal Society of Chemistry
Imprint:   Royal Society of Chemistry
Volume:   Volume 17
Weight:   0.534kg
ISBN:  

9781782625391


ISBN 10:   1782625399
Pages:   256
Publication Date:   28 September 2018
Audience:   Professional and scholarly ,  Professional & Vocational
Format:   Hardback
Publisher's Status:   Active
Availability:   In Print   Availability explained
This item will be ordered in for you from one of our suppliers. Upon receipt, we will promptly dispatch it out to you. For in store availability, please contact us.

Table of Contents

Introduction; Basics of the NMR Experiment; Pulsed Fourier Transform NMR; The NMR Spectrometer; Acquiring 1H and13C Spectra; One-dimensional Pulse Sequences; Two-Dimensional NMR Basics; Two-dimensional Homonuclear Spectroscopy; Heteronuclear Shift Correlation Sequences; Sample Dereplication and Data Archiving; Using Combinations of 2D NMR Spectral Data for Ab Initio Structure Elucidation of Natural Products and Other Unknown Organic Compounds; Avoiding Getting the Wrong Structure; What Does the Future Hold for Small Molecule Structure Elucidation by NMR

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