Mass Spectrometry: Techniques for Structural Characterization of Glycans

Author:   Michael A. Madson (BioLogistics, LLC, Iowa, USA)
Publisher:   Elsevier Science Publishing Co Inc
ISBN:  

9780128041291


Pages:   86
Publication Date:   23 May 2016
Format:   Hardback
Availability:   Manufactured on demand   Availability explained
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Mass Spectrometry: Techniques for Structural Characterization of Glycans


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Author:   Michael A. Madson (BioLogistics, LLC, Iowa, USA)
Publisher:   Elsevier Science Publishing Co Inc
Imprint:   Elsevier Science Publishing Co Inc
Dimensions:   Width: 15.20cm , Height: 1.00cm , Length: 22.90cm
Weight:   0.320kg
ISBN:  

9780128041291


ISBN 10:   0128041293
Pages:   86
Publication Date:   23 May 2016
Audience:   Professional and scholarly ,  Professional & Vocational
Format:   Hardback
Publisher's Status:   Active
Availability:   Manufactured on demand   Availability explained
We will order this item for you from a manufactured on demand supplier.

Table of Contents

• Introduction • Monosaccharide Composition Analysis • Elemental Analysis of MS Ions • Derivatization Techniques • Hydride Addition to Sulfate and phosphate- Chemistry • Instrumentation MALDI-TOF MS API 2000 MS ICP ESI TOF MS • Hydride Insertion Addition Reaction for the Derivatization of Phosphorylated or Sulfated Glycans and the Discernment of Phosphate versus Sulfate Esters • Ester Substitution MS Method The Protocol for the Hydride Addition to the ethanol extract of banana fruit Example of MS2on Hydride added to the ethanol Extract of Banana Fruit Glycan • Glycan Isolation Methods • Other Glycan isolation Methods • Monosaccharide Analysis Acid Hydrolysis • Mass Spectral Carbohydrate Structure Determination Method MS MS/MS (MS2) MSn Proposing Initial Structure Refining Methods for Determining Exact Mass Structure MS Instrumentation Requirements for Discovering Whole Molecule Ions Derivatization Method and Sulfate/Phosphate Discernment Method • References

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Mike Madson is CEO and Senior Research Scientist of BioLogistics, LLC, Iowa, USA

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