Overview

An in-depth analysis of chromatography literature and procedures since 1981 is presented in this publication. Featured is a compre-hensive range of tables relating to the chromatographic separation and determination of amino acids, amines, and their derivatives. Methods of sample preparation and derivatization and methods of detection are described. Included are techniques for the liquid and gas chro-matographic separation of free amino acids and their derivatives, including o-phthalaldehyde, dansyl, and phenylthiolaydantoin deriva-tives. The separation of amino acid enantiomers is also described. This book will be invaluable to chemists, biochemists, and analysts involved in the separation and determination of amino acids or amines and their derivatives.

Full Product Details

Author:   S. Blackburn ,  Joseph Sherma (Lafayette College, Easton, Pennsylvania, USA) ,  Joseph Sherma
Publisher:   Taylor & Francis Inc
Imprint:   CRC Press Inc
Volume:   6
Dimensions:   Width: 21.00cm , Height: 2.30cm , Length: 28.00cm
Weight:   0.566kg
ISBN:  

9780849330667

ISBN 10:   0849330661
Pages:   424
Publication Date:   31 May 1989
Audience:   College/higher education ,  Professional and scholarly ,  Undergraduate ,  Postgraduate, Research & Scholarly
Format:   Hardback
Publisher's Status:   Active
Availability:   In Print  
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Table of Contents

TABLES. Gas Chromatography Tables. Liquid Chro-matography Tables. Thin Layer Chromatography Tables. TECHNIQUES. The Liq-uid Chro-matographic Determination of Free Amino Acids. The Gas Chromatographic Determination of Amino Acids. The Chromato-graphic Separation of Amino Acid Enantiomers. The Liquid Chro-matographic Separation of o-Phthalaldehyde Amino Acid Deriva-tives. The Chromatographic Separation of Phenylthiohy-dantoin Amino Acids. The Chromatographic Separation of Dan-syl Amino Acids. The Chromatographic Separation of Phenylthiocarbamyl Amino Acids. The Chromatographic Separa-tion of Dimethylaminobenzenesulfonyl (DABS)-Amino Acids. The Chromatographic Separation of 4-N,N-Dimethylaminoazoben-zene-4'-thiohydantoin (DABTH)-Amino Acids. The Determination of Proline and Hydrox-yproline by Derivatization with 4-Chloro or 4-Flu-oro-7-Nitrobenzofurazan (NBD-Cl and NBD-F). DETECTION REAGENTS. Detection Meth-ods for Amino Acids and Amines. Summary Tables for Detection Reagents. METHODS OF SAMPLE PREPARATION INCLUDING DERIVATI-ZATION. PRODUCTS AND SOURCES OF CHROMATOGRAPHIC MATERIALS. INDEXES

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Stanley Blackburn, Ph.D., C.Chem., F.R.S.C. Leeds, England

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